Equipment
The Chair of Ceramic Materials Engineering is pleased to support you with problems or projects. If you are interested, please contact our secretariat.
Additive Manufacturing
- Fused Filament Fabrication (FFF) / Fused Deposition Modeling (FDM)Hide
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Fiber™ (Desktop Metal)
- Printing Technologies: Micro Automated Fiber Placement (µAFP)
- Installation space: 310 x 240 x 270 mm³
- Nozzle temperature: max. 500 °C
- Print bed temperature: max. 150 °C
- see news release
INTAMSYS HT Enhanced
- Installation space: 260 mm x 260 mm x 260mm (W x D x H)
- Nozzle temperature: 450 °C
- Installation space temperature: max. 90 °C
- Print bed temperature: max. 160 °C
Creality3D CS-10-S5
- Installation space: 500 mm x 500 mm x 500 mm (W x D x H)
- Nozzle temperature: 240 °C
CooCheer A8
- adapted for filaments with ceramic filler
- Installation space: 220 mm x 270 mm x 240 mm (W x D x H)
- Nozzle temperature: 240 °C
Qidi Tech X-Pro
- Dual extruder
- Installation space: 230 mm x 150 mm x 150 mm (W x D x H)
- Nozzle temperature: 240 °C
- Direct Ink Writing (DIW)Hide
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Anycubic Kossel
- Delta printer for paste printing
- Installation space: diameter 230 mm, height 300 mm
CERAMBOT
- Delta printer for paste printing
- Installation space: diameter 170 mm, height 280 mm
- Stereolithography (SLA)Hide
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Anycubic Photon
- SLA printer for unfilled and filled polymers
- Installation space: 115 mm x 65 mm x 155 mm (W x D x H)
- Post-TreatmentHide
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Anycubic Wash & Cure
- SLA Post-Treatment
Polymaker Polysher
- FDM Post-Treatment for PVB Filaments
Coatings
- ProductionHide
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- Semi-automatic spraying equipment
- Dipping equipment
- Spray booth with spray lance for interior coating
- Coating AnalyticsHide
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- Profilometer: Coating thickness measurement and roughness
- Scratch hardness tester: Lineartester (Erichsen)
- Contact angle measurement (DSA100, Krüss)
Fiber technology
- Fiber productionHide
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- Laboratory spinning plant
- Pilot spinning plant
- Fiber coatingHide
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- Continuous, wet-chemical fiber coating plant
Mechanical characterization
- Universal testing machinesHide
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Universal testing machine Inspekt table blue (Hegewald & Peschke Meß- und Prüftechnik GmbH)
- load cells: 20 N - 5 kN
- Room temperature
- Single fiber tensile test
- Compression test
- 3- and 4-point bending
- Double ring bending test
- Tensile test of ceramic foils
- load cells: 20 N - 5 kN
- Z050TEW high-temperature universal testing machine (ZwickRoell Testing Systems GmbH)
- load cells: 20 N - 50 kN
- Room temperature - 1550 °C (two-zone short furnace up to 1400 °C; three-zone tube furnace up to 1550 °C; air or purge gas)
- Video extensometer at room temperature
- Laser extensometer for longitudinal and transverse strain up to 1550 °C (non-contact, mark-free)
- Single fiber tensile test (RT - 1400 °C)
- 3- and 4-point bending (RT - 1550 °C)
- Tensile test (RT - 1400 °C)
- Compression test (RT - 1550 °C)
- Double ring bending test (RT - 850 °C)
- load cells: 20 N - 50 kN
- Hardness testHide
Microstructure characterization and elemental analysis
- MicroscopyHide
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- Light microscopes
- Scanning electron microscope incl. EDX and EBSD (Zeiss Sigma 300 VP)
- Raman microscope (Bruker Senerra II)
- Elemental analysisHide
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- X-ray diffractometer (Bruker D8 Advance with high temperature chamber up to 1200 °C)
- FT-IR instrument (Bruker Vector 22)
- PreparationHide
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- Cerographic preparation equipment (Struers, hand-held and semi-automatic)
- Variable optical measuring equipmentHide
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- Reflection probe
- Integrating sphere
- div. light sources
- Spectrometer (UV/VIS/NIR, Echelle)
Furnaces
- oxideHide
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- sintering furnaces (Ceram Aix, Nabertherm, oxidizing atmosphere, Tmax=1750 °C)
- various chamber furnaces
- High temperature furnaces (up to 1750 °C)
- calcining furnaces (Fa. Nabertherm, Tmax = 1350 °C, oxidizing atmosphere)
- non-oxideHide
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- Graphitizing furnace (FCT, diameter: 250 mm, height: 300 mm, max. 2400 °C)
- Heraeus tube furnace (nominal temperature: 1100 °C, approx. 9 kW, 380 V, 24 A, 50/60 Hz, heated length: 1 m, Al2O3 ceramic tube (outer diameter: 90 mm, inner diameter approx. 75 mm), operation under protective gas (nitrogen, argon), heating rate: 5 K/min
- Pyrolysis furnace (FCT, diameter: 400 mm, height: 600 mm, 1000 °C)
- Siliconizing furnace (FCT, diameter: 400 mm, height: 500 mm)
- Protective gas tube furnaces for controlled atmosphere including control system
Precursor ceramic
- SynthesisHide
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- Development laboratory for heteroelement inorganic precursors including high vacuum line
- ProcessingHide
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- Glove boxes (Braun company)
Powdered technology
- Powder characterizationHide
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- Particle sizer (Cilas HR 850; 0.1- 600 µm)
- Particle sizer (Anton Paar PSA 1190; 0.04 - 2500 µm in suspension; 0.1 - 2500 µm dry)
- Slurry productionHide
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- Freeze drying plant (ALPHA 1-4 LSC, Martin Christ company)
- Planetary and agitator ball mill
- Vibrating cup mill (Pulverisette 9, Fritsch company)
- Ultrasonic disintegrator
- Fluidized bed reactor (Minibatch, Heinen company)
- Slurry characterization Hide
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- Mobility Meter (Zeta potential; Field ESA, Partikel-Analytik Messgeräte GmbH)
- Rheometer (Anton Paar MCR 702 MultiDrive with furnace up to 600 °C)
- ProductionHide
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- Uniaxial workshop press (ENERPAC, F = 500 kN)
Thermal analysis
- DilatometryHide
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Dilatometer (Netzsch, 402E/7, max. 1500 °C)
- Simultaneous Thermogravimetry - Differential Scanning Calorimetry (STA/TG-DSC)Hide
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- TG and DSC/DTA (Netzsch STA 449 F5 Jupiter)
- DTA/DSC with FT-IR, MS and GC (Netzsch STA 449 F3 Jupiter) including automatic sample changer
Tribology
- TribometerHide
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- Pin-Disc (Waza): Friction coefficient determination, 100 Hz, 1000 N contact pressure
- Brake test standHide
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- In-house design in cooperation with the Chair of Design and CAD
- Up to 1200 kW, area-specific friction power up to 3200 W/mm2
- Speed max = 2500 rpm-1
- Braking force: pneumatic up to 50 kN
- Brake pressures: depending on specimen size (e.g. for 30 x 30 mm² up to 60 MPa)
- Flywheel mass: 800 kg (120 kgm²) and 200 kg (15 kgm²) available
- Tests with constant sliding speed
- Stop-braking tests, i.e. tests with decreasing speed
- Pad size: 10 x 20 x 10 mm³ to 30 x 30 x 10 mm³ (L x W x D, other sizes on request)
- Brake discs: 250 - 1000 mm diameter (other diameters on request)
Composites Manufacturing
- Hot pressHide
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- Fiber composite laboratory with laboratory hot press (heating plate size: 150 x 150 mm², 400 °C)
- Winding technologyHide
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- 4-axis laboratory winding line (XWinder 4X-23)
- Fiber/roving cutting machineHide
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- possible cutting length: 6 mm, 12 mm, 24 mm, 48 mm, 96 mm